Synthesis of Mg-Ferrite nanoparticles via auto combustion method and investigation their structural, morphological and magnetic properties

Authors

  • Ibrahim F. Waheed
  • Faiz M. AL-Abady
  • Baidaa M. Ali

DOI:

https://doi.org/10.25130/tjps.v24i7.458

Abstract

Magnesium ferrite (MgFe2O4) nanoparticles is prepared by sol-gel auto combustion method and calcinated at (200,450, 900) °C. The capping agent was urea and (Mg(NO3)2.6H2O) and (Fe(NO3)3.9H2O) nitrates as sources of metal. X-ray diffraction (XRD) and Fourier transform infrared spectroscopy (FT-IR) characteristic show clear modes of the cubic Mg-ferrite structure formation. Infrared spectrum of metal-oxygen vibration at (703-636) and (574-433) cm−1 show the tetrahedral and octahedral site of Mg-ferrite structure. Scanning Electron Microscope (SEM) images shown pure crystalline microstructure with polyhedral shapes and very small numbers of globular small particles. The crystallite size of Mg-ferrite is calculated using Debye-Scherrer relation and was in the range of 29 nm.

Downloads

Published

2019-12-23

How to Cite

Ibrahim F. Waheed, Faiz M. AL-Abady, & Baidaa M. Ali. (2019). Synthesis of Mg-Ferrite nanoparticles via auto combustion method and investigation their structural, morphological and magnetic properties. Tikrit Journal of Pure Science, 24(7), 52–58. https://doi.org/10.25130/tjps.v24i7.458

Issue

Vol. 24 No. 7 (2019)

Section

Articles

Categories

License

Copyright (c) 2022 Tikrit Journal of Pure Science

Creative Commons License

This work is licensed under a Creative Commons Attribution 4.0 International License.

Tikrit Journal of Pure Science is licensed under the Creative Commons Attribution 4.0 International License, which allows users to copy, create extracts, abstracts, and new works from the article, alter and revise the article, and make commercial use of the article (including reuse and/or resale of the article by commercial entities), provided the user gives appropriate credit (with a link to the formal publication through the relevant DOI), provides a link to the license, indicates if changes were made, and the licensor is not represented as endorsing the use made of the work. The authors hold the copyright for their published work on the Tikrit J. Pure Sci. website, while Tikrit J. Pure Sci. is responsible for appreciate citation of their work, which is released under CC-BY-4.0, enabling the unrestricted use, distribution, and reproduction of an article in any medium, provided that the original work is properly cited.